Chemistry, Physics and Technology of Surface

ISSN 2518-1238 (Online), ISSN 2079-1704 (Print)

The preparation of ceramic composites based on metal nanopowders allows us to change significantly the thermal characteristics of the ceramic matrix, which is important for the creation of heat-conducting ceramics technology.

The work establishes the most efficient method of obtaining nickel nanopowder on a “P-5848” potentiostat by electrolysis of nickel sulfate (NiSO₄) with the addition of boric acid (H₃BO₃), thiourea ((NH₄)₂CS) and nickel(II) chloride (NiCl₂). The synthesis of Ni nanopowder was carried out at a current density from 1.0 to 3.3 A/dm² and at a temperature of 45–65 °C, where a platinum (Pt) plate was chosen as an anode, and the cathode was specially made of especially pure aluminum (Al). The results of the study showed the synthesis of Ni nanopowder with a size of 55 nm in the form of thin scales. Electrochemical reactions at the cathode and anode are also considered in the work.

Several successful experiments were also carried out in the work, which made it possible to develop an economically profitable technology for the synthesis of copper nanopowder by the electrolysis method at 13.3 ampere-hours of current per 1 dm² of the anode surface at a relatively low temperature of the copper sulfate solution (CuSO₄). Copper nanopowder is removed to the bottom of the bath from the anode by impact shaking. An equally successful experiment was carried out, where the cathode was in the form of several copper plates at the distance of 0.8 cm from each other with a voltage between them of 0.775 V, and a current density of 15.3 A/dm² at the temperature of 54 °С in an electrolyte with 45 % H₂SO₄, 8 % Na₂SO₄ and 4 % CuSO₄.

The work contains tables with initial and final data of all experiments on the synthesis of nanopowders by the electrolysis method.

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Semchuk O.Y., Biliuk A.A., Havryliuk O.O. The Kinetic Theory of the Width of Surface Plasmon Resonance Line in Metal Nanoparticles. Springer Proceedings in Physics. 2021. 264: 3. https://doi.org/10.1016/j.apsadv.2021.100057

Ivashchenko V.I., Turchi P.E.A., Shevchenko V.I., Olifan E.I. First-principles study of phase stability of stoichiometric vanadium nitrides. Phys. Rev. B. 2011. 84(17): 174108. https://doi.org/10.1103/PhysRevB.84.174108

Baglyuk G.A., Terekhov V.N., Ternovoi Y.F. Structure and properties of powder austenitic die steels. Powder Metall. Met. Ceram. 2006. 45(7-8): 317. https://doi.org/10.1007/s11106-006-0083-0

Tolochyn O.I., Baglyuk G.A., Tolochyna O.V., Evych Y.I., Podrezov Y.M., Molchanovska H.M. Structure and Physicomechanical Properties of the Fe3Al Intermetallic Compound Obtained by Impact Hot Compaction. Mater. Sci. 2021. 56(4): 499. https://doi.org/10.1007/s11003-021-00456-y

Ivashchenko V.I., Vepřek S. First-principles molecular dynamics study of the thermal stability of the BN, AlN, SiC and SiN interfacial layers in TiN-based heterostructures: Comparison with experiments. Thin Solid Films. 2013. 545: 391. https://doi.org/10.1016/j.tsf.2013.08.047

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Baglyuk G.A., Ivasyshyn O.M., Stasyuk O.O., Savvakin D.G. Sintered metals and alloys: The effect of charge component composition on the structure and properties of titanium matrix sintered composites with high-modulus compounds. Powder Metall. Met. Ceram. 2017. 56(1-2): 59. https://doi.org/10.1007/s11106-017-9870-z

Baglyuk G.A., Sosnovskii L.A., Volfman V.I. Effect of carbon content on the properties of sintered steels doped with manganese and copper. Powder Metall. Met. Ceram. 2011. 50(3-4): 189. https://doi.org/10.1007/s11106-011-9317-x

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Baglyuk G.A., Poznyak L.A. Sintered wear-resistant iron-based materials. I. Materials fabricated by sintering and impregnation. Poroshkovaya Metallurgiya. 2001. 1-2: 44.

Sizonenko O.N., Baglyuk G.A., Taftai E.I., Zaichenko A.D., Lipyan E.V., Torpakov A.S., Zhdanov A.A., Pristash N.S. Dispersion and carburization of titanium powders by electric discharge. Powder Metall. Met. Ceram. 2013. 52(5-6): 247. https://doi.org/10.1007/s11106-013-9520-z

Ivashchenko V.I., Veprek S., Turchi P.E.A., Shevchenko V.I., Leszczynski J., Gorb L., Hill F. First-principles molecular dynamics investigation of thermal and mechanical stability of the TiN(001)/AlN and ZrN(001)/AlN heterostructures. Thin Solid Films. 2014. 564: 284. https://doi.org/10.1016/j.tsf.2014.05.036

Baglyuk G.A., Napara-Volgina S.G., Vol'Fman V.I., Mamonova A.A., Pyatachuk S.G. Thermal synthesis of Fe-B 4C powder master alloys. Powder Metall. Met. Ceram. 2009. 48(7-8): 381. https://doi.org/10.1007/s11106-009-9156-1

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