Хімія, фізика та технологія поверхні, 2017, 8 (3), 271-288.

Вплив механохімічного модифікування на властивості порошків оксиду і оксигідроксиду олова(iv)



DOI: https://doi.org/10.15407/hftp08.03.271

S. V. Khalameida, M. M. Samsonenko, J. Skubiszewska-Zięba, O. I. Zakutevskyy, L. S. Kuznetsova

Анотація


Шляхом механохімічної обробки модифіковано зразки порошків низькодисперсного оксиду олова(IV) та високодисперсного оксигідроксиду олова(IV). Фізико-хімічні властивості всіх зразків досліджені за допомогою ДТА, РФА, ІЧ-спектроскопії з Фур’є перетворенням, адсорбції-десорбції азоту, UV-Vis-спектроскопії. Оцінку фотокаталітичної активності проводили шляхом деградації родаміну Б та сафраніну Т у водному середовищі. Встановлено, що в результаті механохімічної обробки всіх зразків формується мезо-макропорувата структура. Спостерігається залежність ефективності фотокаталітичної деградації родаміну Б від дисперсності, наявності дефектів на поверхні каталізатора та його електронної структури.

Ключові слова


оксид і оксигідроксид олова(IV); механохімічна обробка; порувата структура; родамін Б; фотокаталітична активність

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DOI: https://doi.org/10.15407/hftp08.03.271

Copyright (©) 2017 S. V. Khalameida, M. M. Samsonenko, J. Skubiszewska-Zięba, O. I. Zakutevskyy, L. S. Kuznetsova

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