ХІМІЯ, ФІЗИКА ТА ТЕХНОЛОГІЯ ПОВЕРХНІ

ISSN 2518-1238 (Online), ISSN 2079-1704 (Print)

Мета науководослідної роботи полягала у піролітичному синтезі вуглецевих нанотрубок прямого та спірального типу приблизно однакового діаметра, а також їхній комплексний аналіз. Для вирішення поставленої задачі була створена нова установка для піролітичного синтезу вуглецевих наноструктур (ВНС), з реактором синтезу, який для кожного процесу синтезу може мати свій кут відносно класичного горизонтального положення вісі реактора. Даний реактор дозволив розробити метод отримання конгломератів спіралеподібних багатостінних вуглецевих нанотрубок (СБВНТ) діаметром 15–60 нм та синтезувати прямі багатостінні вуглецеві нанотрубки (ПБВНТ) діаметром від 5 до 60 нм.

Дослідженя піролітичного синтезу вуглецевих наноструктур на вертикальному реакторі дозволяє відпрацювати технологію цілеспрямованого синтезу нанотрубок, що мають спіральну форму з певним діаметром та кроком витку.

В рамках роботи також розглянутий та запропонований новий механізм формування спіральних багатостінних вуглецевих нанотрубок, що важливо для їхнього подальшого промислового синтезу та використання їх в композитах на їхній основі.

Запропонована схема умов синтезу вуглецевих наноструктур піролітичним методом.

У роботі проводили термоаналіз, що зафіксував присутність двох різних структур з низькою термостійкістю (ймовірно, аморфний вуглець та вищі вуглеводні). При використанні скануючої і просвічувальної електронної мікроскопії було зафіксовано утворення у вертикальному положенні реактора спіралеподібних нановолокон діаметром 15–60 нм, а у горизонтальному положенні - прямих і злегка вигнутих БВНТ з діаметром нановолокна від 5 до 60 нм. Раманівською спектроскопією підтверджує в обох продуктах синтезу наявність багатошарового вуглецевого трубчастого формування, тобто БВНТ.

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